AMS2700E

更新时间:2023-07-21 22:27:55 阅读: 评论:0

__________________________________________________________________________________________________________________________________________ SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences.  The u of this report is entirely voluntary, and its applicability and suitability for any particular u, including any patent infringement arising therefrom, is the sole responsibility of the ur.”
SAE reviews each technical report at least every five years at which time it may be reaffirmed, revid, or cancelled.  SAE invites your written comments and suggestions. Copyright © 2011 SAE International
All rights rerved. No part of this publication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwi, without the prior written permission of SAE.
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www.sae/technical/standards/AMS2700E
AEROSPACE
MATERIAL
SPECIFICATION
AMS2700 REV. E
Issued 2000-03
tae是谁Revid 2011-11
Superding AMS2700D
A MS-QQ-P-35
QQ-P-35
Passivation of Corrosion Resistant Steels
RATIONALE
AMS2700E is issued to incorporate all changes approved by AMS Committee B by 28 day Limited Scope Ballot clod on 6/14/2011 and which were intended to be reflected in AMS2700D but some of which were inadvertently omitted. A complete list of each of the changes is listed in 8.17.
1. SCOPE
1.1 Purpo
This specification covers the requirements for a process to assure removal of free iron or other less noble contaminants from the surfaces of corrosion resistant steel parts.
1.2 Application
The process defined in this specification have been ud typically to dissolve tramp metallic elements from the surfaces of corrosion resistant steels to improve their corrosion resistance, but usage is not limited to such applications.
1.3 Classification
新东方英语教师培训
1.3.1 Methods
Passivation methods covered by this specification are as follows:
Method 1 -  P assivation in Nitric Acid
扬州补习Method 2 -  P assivation in Citric Acid
Method 1 shall be ud unless Method 2 is authorized by the cognizant engineering organization.
1.3.2 Types
The following types may be specified for Method 1:
Type 1 Low Temperature Nitric Acid with Sodium Dichromate
Type 2 Medium Temperature Nitric Acid with Sodium Dichromate
Type 3 High Temperature Nitric Acid with Sodium Dichromate
Type 4 40% Nitric Acid for Free Machining Steels
Type 5 Anodic, for High Carbon Martensitic Steels
Type 6 Low Temperature Nitric Acid
Type 7 Medium Temperature Nitric Acid
Type 8 Medium Temperature, High Nitric Acid Concentration
Where no type is specified, the processor may u any of the listed types that meet the requirements given herein.
1.3.3 Class
互动英文Passivation verification class are as follows:
coverage
1
1.3.3.1 Class
The following types of parts shall be lected for testing in accordance with 4.3.1.
1.3.3.1.1 Fasteners, including nuts, bolts, washers, rivets and related hardware where a test frequency is not defined in
the procurement documents.
1.3.3.1.2 Standard parts defined by drawings labeled AN, MS, NAS or similar where frequency of test is not otherwi
defined.
1.3.3.1.3 When specified by purchar.
2
1.3.3.2 Class
Frequency of corrosion testing shall be one part per lot.
1.3.3.3 Class
3
Frequency of testing shall be on a periodic basis.
4
1.3.3.4 Class
Parts for which AMS-QQ-P-35 or QQ-P-35 is specified shall be acceptance tested in accordance with 4.3.4.
1.3.3.5 When no class is specified and neither 1.3.3.1 nor 1.3.3.4 apply, class 2 shall apply.
1.4 Safety - Hazardous Materials
While the materials, methods, applications, and process described or referenced in this specification may involve the u of hazardous materials, this specification does not address the haz
ards which may be involved in such u. It is the sole responsibility of the ur to ensure familiarity with the safe and proper u of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved.
2. APPLICABLE DOCUMENTS
The issue of the following documents in effect on the date of the purcha order forms a part of this specification to the extent specified herein. The supplier may work to a subquent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superding document has been specified, the last published issue of that document shall apply.
2.1 SAE Publications
Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.
C hemical Process Test Specimen Material
AS2390
2.2 ASTM Publications
Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.
ASTM B 117 Operating Salt Spray (Fog) Testing Apparatus
ASTM D 1193 Reagent Water
3. REQUIREMENTS
3.1 Procedure
3.1.1 Passivation shall be performed only on surfaces free from water breaks and visible rust or scale. See 8.8.
3.1.2 Method 1 - Passivation in Nitric Acid
3.1.2.1
P assivation shall be accomplished by immersion in a bath in accordance with Table 1. When permitt
ed by the cognizant engineering organization, other nitric acid solutions may be ud. See 8.13.
3.1.2.2 When a specific passivation type is not specified, Table 4 may be consulted for recommended types.
TABLE 1 - METHOD 1 PASSIVATION TYPES
Type Feature Value
1 Bath Composition 20 to 25% by volume of HNO3
2 to 3% by weight Na2Cr2O7·2H2O
Bath temperature 70 to 90 °F (21 to 32 °C)
Immersion time 30 minutes minimum
2 Bath Composition 20 to 25% by volume of HNO3
2 to 3% by weight Na2Cr2O7·2H2O
Bath temperature 120 to 130 °F (49 to 54 °C)
Immersion time 20 minutes minimum
3 Bath Composition 20 to 25% by volume of HNO3
2 to 3% by weight Na2Cr2O7·2H2O
Bath temperature 145 to 155 °F (63 to 68 °C)
Immersion time 10 minutes minimum
4 Bath Composition 38 to 42% by volume of HNO3
2 to 3% by weight Na2Cr2O7·2H2O
Bath temperature 70 to 120 °F (21 to 49 °C)
Immersion time 30 minutes minimumtowns
5 Bath Composition 20 to 25% by volume of HNO3
2 to 3% by weight Na2Cr2O7·2H2O
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Bath temperature 70 to 90 °F (21 to 32 °C)
Immersion time    2 minutes minimum
Voltage Part anodic at 3 to 5 volts
6 Bath Composition 25 to 45% by volume HNO3
Bath temperature 70 to 90 °F (21 to 32 °C)
Immersion time 30 minutes minimum
7 Bath Composition 20 to 25% by volume HNO3
Bath temperature 120 to 140 °F (49 to 60 °C)
Immersion time 20 minutes minimum
8 Bath Composition 45 to 55% by volume HNO3
Bath temperature 120 to 130 °F (49 to 54 °C)
Immersion time 30 minutes minimum
NOTE:  Nitric acid concentration shown is by volume of 42° Baume
(sp. gr. 1.4) nitric acid.  See 8.12.
3.1.3 Method 2 - Passivation in Citric Acid
Composition
3.1.3.1 Bath
Parts shall be immerd in an aqueous solution of 4 to 10 weight percent citric acid, with additional wetting agents and inhibitors as applicable.
Conditions
3.1.3.2 Operating
3.1.3.2.1 Temperature
Bath temperature shall be 70 to 160 °F (21 to 71 °C) with an immersion time of not less than 4 minutes for baths operating over 140 °F (60 °C), not less than 10 minutes for baths operating in the 120 to 140 °F (49 to 60 °C) range, not less than 20 minutes for baths operating in the range of 100 to 119 °F (38 to 48 °C) or not less than 30 minutes for baths operating below 100 °F (38 °C).
Rin
3.1.4 Final
Immediately after removal from the passivating solution the parts shall be thoroughly rind.  Final rin shall be carried out in clean water.  See 8.14.
3.1.5 Post
Treatment
When a post treatment is specified, after rinsing, parts made from ferritic, martensitic and precipitation hardening steels shall be immerd in a solution containing 4 to 6% by weight of sodium dichromate dihydrate (Na2Cr2O7·2H2O) at 140 to 160 °F (60 to 71 °C) for 1 hour, rind, and dried.  See 8.2.
3.2 Properties
takkoResistance
available什么意思3.2.1 Corrosion
Except for parts containing 0.85% carbon or more (such as AISI 440C), parts shall meet one of the following conditions, or, when specified, a test method in Appendix A.
3.2.1.1 Humiditycolour
Parts shall be free from visible red rust after exposure to 95% minimum relative humidity at 100 to 115 °F (38 to 46 °C) for not less than 24 hours.
Immersion
3.2.1.2 Water
Parts shall be free from visible red rust after alternately immersing in  reagent water (ASTM D 1193 Type IV) for 1 hour and allowing to dry in room temperature air for 1 hour, until 24 hours (12 cycles) have elapd.  See 8.15.
3.2.1.3 When specified or when permitted by the cognizant engineering organization, (1) for austenitic steels of the
AISI 200 or AISI 300 ries and (2) for precipitation hardened steels and ferritic steels containing more than 16% chromium, one of the following requirements shall be met in lieu of humidity or immersion testing:
3.2.1.3.1 Copper Sulfate Test
Parts shall be swabbed with or immerd in a test solution containing 8 grams of copper sulfate (CuSO4·5H2O) and 2 to 3 milliliters of sulfuric acid (H2SO4, sp. gr. 1.84) in 500 milliliters of reagent water in accordance with ASTM D 1193 Type IV, keeping the surface wet for not less than 6 minutes. Rin and dry the surface without disturbing any deposits. A copper colored deposit indicates the prence of unacceptable free iron. The effectiveness of copper sulfate solutions shall be validated by one of the following methods:
a. Periodic chemical analysis in accordance with 4.2.2.1
b. Verification before u. Test specimens of any convenient size, made from materials in accordance with AS2390
reprenting transformation hardening steels and properly cleaned, shall exhibit a copper-colored deposit when subjected to the test above.
Spray
3.2.1.3.2 Salt
Parts shall withstand exposure to 2 hours minimum in a salt spray environment operated in accordance with ASTM B 117. Parts shall not show evidence of red rust following completion of the test.
3.2.2 Surface
Appearance
After completion of processing, there shall be no evidence of etching, pitting, smutting, frosting, dimensional changes, or other chemical attack on the parts. However, loss of temper color when Method 2 is ud is acceptable.

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