Data File:20140701-lzy08
Original Data Path:D:\GC-MSdata\03-quence data\201407-lzy Current Data Path:D:\GC-MSdata\03-quence data\201407-lzy Sample Type:
Unknown
Sample ID:Trayholder 1:Slot3:8Sample Name:Operator:
ISQ130253Acquisition Date:07/01/14 11:13:43 AM Run Time(min):10.07
Comments:
Vial:Trayholder 1:Slot3:8Injection Volume(µl): 1.00Scans:
2963Low Mass(m/z):33High Mass(m/z):400Sample Volume(µl):0.00Sample Weight:0.00
ISTD Amount:0.000Calibration Level:Dilution Factor:
1.00
Instrument Method:
D:\GC-MSdata\01-instrument method\201405\20140520-4-lzy.m eth Original Processing Method:
Current Processing Method:N/A Calibration File:N/A Instrument Software Version: 1.1.0.53Instrument Name:
ISQ Instrument Model:
ISQ
Instrument Serial Number:1211107
Instrument Hardware Version:210.0.77.17
Barcode:
Barcode Status:
Barcode Not Read
RT:0.00 - 10.11
12
3
4
567
8
9
内部审计制度10
Time (min)
05101520253035404550556065
707580859095100R e l a t i v e A b u n d a n c e
6.14
2.18
1.39
7.314.64
9.258.303.48
5.61
0.70
NL:2.53E8TIC MS 20140701-lzy08
0.0521373.1813465.89 0.1732342.7623218.17 0.30218388.4345250.89 0.4348069.0223484.51 0.4949480.8215101.30 0.7052868.4618420.58 0.7426591.8918768.97 0.7819014.3612140.39 0.8231049.5917955.71 0.8819268.3712271.64
0.9724154.5814330.14
1.0554880.8232646.44 1.1985487.3821454.57 1.2981173.9534831.56 1.398349348.572673841.72 1.6614519539.713098655.99 1.7911135695.87326397
2.16
1.9013178435.553615241.05
2.00295674.84165449.40 2.0631901.201905
食品安全考试3.07 2.1931511322.4310115872.17 2.335024271.022056302.79 2.401236862.47539856.66 2.511270138.91328275.63 2.683812911.061104955.95 2.8430569.001479
4.88
2.916823
3.9936110.30
3.031123981.82291132.48 3.16289241.0465289.24 3.3031681.652467
4.26 3.3915952
5.9742319.59 3.47102775.7133650.63 3.5118235.5614863.56 3.5985270.0633117.14 3.6545721.9627204.63 3.7380005.5731815.42 3.804173
6.7424321.49 3.8557788.4034893.43
3.92323661.84108539.81
4.04647200.14177794.83 4.1867426.3139630.57 4.24113739.0042877.55 4.32128543.553524
5.91 4.36175007.7442283.14 4.5138344.2121469.69 4.5645324.0725410.19 4.64717548.77202183.25 4.7362105
6.73167633.67 4.83168360.6161641.19
4.92363394.0894514.16
5.0719390
6.5637555.64 5.156083
7.3429374.42 5.25125123.0831994.00 5.3698362.8327174.72 5.4576844.5927920.60 5.58143853.4929304.76 5.6684051.6929400.48 5.7477351.3226052.42 5.8284312.6520049.18 5.9058865.7822240.70
5.992441
6.7811983.59
6.141035782358.67229009603.08 6.46106295.6444878.28 6.5339399.0227545.08
6.6142299.5919156.686.6636259.6822970.876.7628169.6421765.856.8188111.9225161.536.961050825.71311361.19
7.108463
8.3331041.717.1935328.1019202.937.311239818.74356664.467.47138726.8042273.907.731075221.48209743.307.8616403.4711855.617.9148818.4027680.507.9516231.0213772.328.0358031.1031475.438.0886568.7930447.688.1571837.5729440.208.2337591.9323897.038.3077557.732619电脑怎么上外网
9.038.37142062.0736901.348.4958669.4232835.688.56142810.8828794.258.6866068.7934775.708.8147052.7925883.808.8747447.7422333.848.9726408.7112457.989.0034572.2818660.779.0656597.0725330.369.1696931.7426663.269.2135869.0423323.619.2526897.0322365.559.3286075.2633830.929.3763028.2824206.029.46114354.7125892.119.5423387.2916033.769.5819187.2218194.909.83
5373142.45
1332118.13
20140701-lzy08#6RT:0.05AV:1AV:5SB:12 -1-4 8-13NL:1.99E4F:{0,0} + c EI Full ms [33.00-400.00]
50
100
150
200
250
300
350
m/z
102030405060708090100R e l a t i v e A b u n d a n c
e
57.1
71.1
143.2
106.1
207.2236.2264.1
294.1342.0375.9
RT:0.03 - 0.58SM:15G
Time (min)
R e l a t i v e A b u n d a n c e
Compound Name
Cas #Molecular Formula
Probability
Benzeneethanamine,
2,5-difluoro-á,3,4-trihydroxy-N-methyl-
152434-78-1
C9H11F2NO3
20.19
Hit Spectrum
Delta Compound Structure
错缘m/z
1020304050607080
90100R e l a t i v e A b u n d a n c e
44
4578
57
124106173159199219100
-100-500
50
40
435777
207294
Benzeneethanamine, 2,5-difluoro-á,3,4-trihydroxy-N-methyl-Formula C9H11F2NO3, MW 219, CAS# 152434-78-1, Entry# 145283,6-Difluoro-4-[1-hydroxy-2-(methylamino)ethyl]-1,2-benzenediol #
F HO
HO
F
OH
NH
20140701-lzy08#40RT:0.17AV:1AV:5SB:12 33-38 42-47NL:1.29E4F:{0,0} + c EI Full ms [33.00-400.00]
m/z
1020
3040506070
8090100R e l a t i v e A b u n d a n c
e
77.1
明星减肥
96.3
130.9
165.1
282.1
227.3
333.2
376.4
RT:0.03 - 0.68SM:15G
Time (min)
R e l a t i v e A b u n d a n c e
Compound Name
Cas #Molecular Formula
Probability
2,4,6,8,10-Tetradecapentaenoic acid,
9a-(acetyloxy)-1a,1b,4,4a,5,7a,7b,8,9,9a-dec ahydro-4a,7b-dihydroxy-3-(hydroxymethyl)-1,1,6,8-tetramethyl-5-oxo-1H-cyclopropa[3,
4]benz[1,2-e]azulen-9-yl ester,
[1aR-(1aà,1bá,4aá,7aà,7bà,8à,9á,9aà)]-
77550-17-5
C36H46O8
18.28
Hit Spectrum
Delta Compound Structure
m/z
1020304050607080
90100R e l a t i v e A b u n d a n c e
78
18
79149
218222
389606
446588100
-100-500
50
77
96186
Formula C36H46O8, MW 606, CAS# 77550-17-5, Entry# 43714
HO
HO
O新年台词
O
O
OH
O
O
20140701-lzy08#80RT:0.30AV:1AV:5SB:12 73-78 82-87NL:1.00E4F:{0,0} + c EI Full ms [33.00-400.00]
50
100
150
200
250
300
350
m/z
10
203040506070
8090100R e l a t i v e A b u n d a n c
e
65.1
101.1
259.2
191.2
159.2
323.2
356.5
223.3
392.0
RT:0.03 - 0.89SM:15G
Time (min)
R e l a t i v e A b u n d a n c e
Compound Name Cas #Molecular Formula
Probability
Ethyl iso-allocholate
NA
C26H44O5
21.51
Hit Spectrum
Delta Compound Structure
炖菜大全家常菜
m/z
1020304050607080
90100R e l a t i v e A b u n d a n c e
43555769
8183
107121145
149400
253382272
197401
100
-100
-50
50
4044
6586
323
Ethyl iso-allocholate
Formula C26H44O5, MW 436, CAS# NA, Entry# 6654
Ethyl 3,7,12-trihydroxycholan-24-oate #
HO OH
OH
O
O
20140701-lzy08#117RT:0.43AV:1AV:5SB:12 110-115 119-124NL:3.79E3F:{0,0} + c EI Full ms [33.00-400.00]
50
100
150
200
250
300
350
m/z
10203040
506070
8090100R e l a t i v e A b u n d a n c e
56.1
98.1
放松的音乐
69.1
121.0
167.1
192.0
265.1
332.4
239.7
385.3
RT:0.03 - 0.97SM:15G
Time (min)
R e l a t i v e A b u n d a n c e
Compound Name
Cas #Molecular Formula
Probability
N-[4-(4-Chlorophenyl)isothiazol-5-yl)-1-me
thylpiperidin-2-imine NA C15H16ClN3S 9.48
