PREPARATION AND CHARACTERIZATION OF MAGNESIUM CHROMITE AND MAGNESIUMh61主板支持什么cpu
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期刊名称: Chemical Engineering Communications炖青鱼
作者: Willey, Ronald J.,Noirclerc, Patrick,Busca, Guido
妹妹的奶水年份: 2012年
期号: 第1期
麦克勒姆关键词: Aerogels;Sol-Gel;Binary;Oxides;Ferrites;Chromites;Fine;Particle;Powders
摘要:A supercritical drying process has been ud to prepare MgO-Cr2O3, and MgO-Fe2O3 powders from a mixture of magnesium acetate and the metallic acetylacetonates hydrolyzed in a methanolic solvent. The resultant aerogels have small particle sizes in the range of 10 to 20 nm and high surface areas in the range of 50 to 250 m2sol;g. After removal from the autoclave, characterization by X-ray diff上下一体打一字
raction (XRD) showed that the MgO-Cr2O3, was amorphous and that the MgO-Fe2O3 was readily in the form of a spinel structure for magnesioferrite (MgFe2O4). Fourier transform infrared spectroscopy (FTIR) and thermogravimetric and differential Ihermal analys (TG-DTG-DTA) showed a high level of retained surface methoxy and carboxylate species for the MgO-Cr2O3 aerogel (lover 40% by weight). The MgO-Fe2O4, on the otherhand, had less than 10%
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